Environmental Sampling and Analysis for Metals

Determination of metals is a major part of the work of environmental testing laboratories. EPA and DEP methodology releases provide information only for selected areas of metals sampling and analysis, and their language makes them unsuitable for teaching and training purposes. Environmental Sampling...

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Những tác giả chính: Csuros, Maria, Csuros, Csaba
Định dạng: Sách
Ngôn ngữ:English
Được phát hành: CRC Press 2009
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Truy cập trực tuyến:http://scholar.dlu.edu.vn/thuvienso/handle/DLU123456789/1015
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Thư viện lưu trữ: Thư viện Trường Đại học Đà Lạt
id oai:scholar.dlu.edu.vn:DLU123456789-1015
record_format dspace
institution Thư viện Trường Đại học Đà Lạt
collection Thư viện số
language English
topic Environmental Sciences
spellingShingle Environmental Sciences
Csuros, Maria
Csuros, Csaba
Environmental Sampling and Analysis for Metals
description Determination of metals is a major part of the work of environmental testing laboratories. EPA and DEP methodology releases provide information only for selected areas of metals sampling and analysis, and their language makes them unsuitable for teaching and training purposes. Environmental Sampling and Analysis for Metals is a comprehensive and easy-to-read text for laboratory technicians and analytical chemists who need a guide for analyzing metals in environmental samples and a reference for analytical and quality control procedures. The book provides both theoretical and practical applications in metals analysis of environmental samples and incorporates the latest in analytical techniques, instrumentation, and regulations. Topics include sample collection, preservation, step-by-step analytical procedures, complete QA/QC requirements, data validation, and more. It also provides an overview of the occurrence, source, and fate of metallic substances in the environment, as well as their control by regulations and standards. Furthermore, the authors provide guidelines to help you prepare and understand reports. The analytical methods presented in Environmental Sampling and Analysis for Metals will be useful to anyone who produces, uses, or evaluates analytical data, and will be a valuable tool in environmental education and training programs.
format Book
author Csuros, Maria
Csuros, Csaba
author_facet Csuros, Maria
Csuros, Csaba
author_sort Csuros, Maria
title Environmental Sampling and Analysis for Metals
title_short Environmental Sampling and Analysis for Metals
title_full Environmental Sampling and Analysis for Metals
title_fullStr Environmental Sampling and Analysis for Metals
title_full_unstemmed Environmental Sampling and Analysis for Metals
title_sort environmental sampling and analysis for metals
publisher CRC Press
publishDate 2009
url http://scholar.dlu.edu.vn/thuvienso/handle/DLU123456789/1015
_version_ 1757673332032929792
spelling oai:scholar.dlu.edu.vn:DLU123456789-10152009-10-12T07:25:37Z Environmental Sampling and Analysis for Metals Csuros, Maria Csuros, Csaba Environmental Sciences Determination of metals is a major part of the work of environmental testing laboratories. EPA and DEP methodology releases provide information only for selected areas of metals sampling and analysis, and their language makes them unsuitable for teaching and training purposes. Environmental Sampling and Analysis for Metals is a comprehensive and easy-to-read text for laboratory technicians and analytical chemists who need a guide for analyzing metals in environmental samples and a reference for analytical and quality control procedures. The book provides both theoretical and practical applications in metals analysis of environmental samples and incorporates the latest in analytical techniques, instrumentation, and regulations. Topics include sample collection, preservation, step-by-step analytical procedures, complete QA/QC requirements, data validation, and more. It also provides an overview of the occurrence, source, and fate of metallic substances in the environment, as well as their control by regulations and standards. Furthermore, the authors provide guidelines to help you prepare and understand reports. The analytical methods presented in Environmental Sampling and Analysis for Metals will be useful to anyone who produces, uses, or evaluates analytical data, and will be a valuable tool in environmental education and training programs. Introduction to Metals Introduction to Elements Periodic Table of Elements Properties of Metals, Nonmetals, and Metalloids Early History of Metal Use Sources of Metals and Their Compounds Sources of Metal Pollution Discussion of the Metallic Elements Representative Elements Transition Metals Metalloids Heavy Metals Metallic Substances Essential to Life Toxicity of Metals General Discussion of Toxicity Metal Toxicity Toxic Effects of Selected Representative Metals Toxicity of Selected Transition Metals Toxicity of Selected Metalloids Standards Related to Metallic Pollutants Environmental Law Drinking Water Standards Surface Water Standards Agriculturally Used Waters Industrial Waters Waste Characterization Hazardous Waste Characterization Air Pollution and Control ISO 14001 and Environmental Law Fundamentals of Spectroscopy Early History of the Nature of the Light Electromagnetic Radiation Continuous and Line Spectra Absorption and Emission Beer's Law Atomic Spectroscopy Techniques Molecular Spectrophotometry Molecular Absorption and Color Molecular Absorption Spectrophotometry Single-Beam and Double-Beam Spectrophotometer Type of Spectrophotometers Summary of Molecular Spectrophotometry Spectrophotometer Calibration Performance Check of UV/Vis and IR Spectrophotometer Maintenance of the UV/Vis and IR Spectrophotometer Atomic Absorption Spectrometry Introduction Steps in the Atomic Absorption Process Atomic Absorption Spectrophotometer Components Single- and Double-Beam Instruments Atomic Absorption Measurement Terms Techniques in AAS Measurements Interference in AAS Techniques Safety in AAS Work Quality Control Maintenance of AA Spectrophotometers AAS Performance Checks Sample Collection and Sample Preparation Direct Aspiration or Flame Atomic Absorption Spectrometry (FAAS) Principle Direct Air-Acetylene Flame Method Direct Nitrous Oxide-Acetylene Flame Method Interferences, Safety and Quality Control Requirements of FAAS Maintenance of FAA Performance Check of FAAS Graphite Furnace Atomic Absorption Spectrometry General Discussion Apparatus Analysis by Graphite Furnace Spectrophotometer Interferences in the Graphite Furnace Stabilized Temperature Platform Furnace (STPF) Quality Control Requirements Maintenance of Graphite Atomic Absorption Spectrophotometer Performance Check of Graphite Atomic Absorption Spectrophotometer Cold-Vapor Atomic Absorption Spectrometry General Discussion Apparatus Procedure Interference Quality Control Requirements Calculations and Reporting Safety Hydride-Generation Atomic Absorption Technique Principles Application Apparatus and Materials Interferences Sample Collection, Preservation, and Handling Preparation of Samples and Standards for Total Arsenic and Selenium Procedure Quality Control Requirements Inductively Coupled Plasma Atomic Emission Spectroscopy Atomic Emission Spectroscopy (AES) General Characteristics of ICP-AES ICP-AES Instrumentation Interferences in ICP-AES Reagents and Standards Procedure Quality Control Quality Control in Metals Analysis General Discussion Glassware Used in Metals Analysis Chemicals Laboratory-Pure Water Field Quality Control Instrument Calibration Instrument Performance Check Laboratory QC Checks Detection Limits Accuracy and Precision Sample Collection for Metals Analysis General Considerations in Sampling Automatic Samplers Sample Containers Sample Preservation Special Sampling Procedures Holding Time Field Records Field Quality Control Sample Collection from Different Matrices Sample Preparation for Metal Analysis General Discussion Digestion Procedures for Metals Acid Digestion for Total and Dissolved Metals Acid Digestion of Aqueous Samples and Extracts for Total Metals by FAAS and ICP Analyzer Acid Digestion of Aqueous Samples and Extracts for Total Metals by GrAAS Sample Preparation for Arsenic and Selenium determination by GrAAS Sample Preparation for Silver Determination Sample Preparation for Antimony Determination Sample Preparation for Mercury Determination Acid Digestion of Sediments, Sludges, and Soils for Metals Analysis Dissolution Procedure for Oils, Greases, and Waxes Sample Preparation for Hexavalent Chromium (Chelation/Extraction) Extraction Procedure (EP) Toxicity Extraction Procedure for Oily Wastes Documentation during Sample Preparation Disposal of Samples, Digestates, Extracts, and Other Wastes Converting Raw Data into Reportable Form Responsibilities of the Analyst Calculations for Final Values Records for Raw and Calculated Data Evaluation and Approval of Analytical Data Reporting Analytical Data Required Documentation Significant Figures in Analytical Reports Units Used to Express Analytical Results Confidence Interval Report Format Selected Methods for Determination of Metals in Environmental Samples Methodology Aluminum Antimony Arsenic Barium Beryllium Bismuth Cadmium Calcium Chromium Hexavalent Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Mercury Molybdenum Nickel Potassium Selenium Silver Sodium Thallium Tin Vanadium Zinc Laboratory Safety Rules Laboratory Hazards Safe Handling of Compressed Gases Stockroom Safety Rules Summary of Laboratory Safety Rules Appendices Operation of Mass Spectrophotometer Silicon Chips Lasers Metals and Plants Toxicity and Cyanide Components of Nucleic Acid Polarized Light Stock Metal Solutions Calculation for Solid Matrices Plasma Sohxlet Extraction SI Units and Conversion Factors References Index 2009-10-12T07:25:37Z 2009-10-12T07:25:37Z 2002 Book 978156670572 http://scholar.dlu.edu.vn/thuvienso/handle/DLU123456789/1015 en application/octet-stream CRC Press