STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES

We synthesized 0-3 type (1-x)PbTiO3-xNiFe2O4 (x = 0.0-0.5) multiferroic composites with two independently crystallized parent phases by the sol-gel method. Structural, surface morphology, vibrational, optical, and magnetic characteristics were investigated by X-ray diffraction (XRD), SEM, Raman scat...

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Những tác giả chính: Pham, Do Chung, Le, Thi Mai Oanh, Nguyen, Van Minh
Định dạng: Bài viết
Ngôn ngữ:English
Được phát hành: Trường Đại học Đà Lạt 2023
Truy cập trực tuyến:https://scholar.dlu.edu.vn/thuvienso/handle/DLU123456789/114424
https://tckh.dlu.edu.vn/index.php/tckhdhdl/article/view/911
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spelling oai:scholar.dlu.edu.vn:DLU123456789-1144242023-10-27T14:46:37Z STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES Pham, Do Chung Le, Thi Mai Oanh Nguyen, Van Minh We synthesized 0-3 type (1-x)PbTiO3-xNiFe2O4 (x = 0.0-0.5) multiferroic composites with two independently crystallized parent phases by the sol-gel method. Structural, surface morphology, vibrational, optical, and magnetic characteristics were investigated by X-ray diffraction (XRD), SEM, Raman scattering, UV-vis absorption, and magnetization (M-H) measurements, respectively. The XRD result showed that the lattice parameter a of the PbTiO3 (PTO) phase decreased while lattice parameter c increased after compositing, leading to a decrease in the tetragonal ratio c/a. SEM images indicated that the NiFe2O4 (NFO) crystals that crystallized later are small and adhere to the surface of the large PTO particles. The strong cohesion between the two components was also revealed by the gradual shift of the Raman peaks to the lower wavelength and the reduction of the Raman intensity as the NFO content increased. The UV-vis absorption result showed the co-absorption spectra of the parent phases in the composites. Magnetization curves presented a sharp increase in saturation magnetization MS with NFO content from 0.014 emu/g for the PTO sample to 14.360 emu/g for the composite containing 50 mol% NFO. This study indicates an effective method in the search for multilayer composites. 2023-03-04T08:26:02Z 2023-03-04T08:26:02Z 2021 Article 0866-787X https://scholar.dlu.edu.vn/thuvienso/handle/DLU123456789/114424 https://tckh.dlu.edu.vn/index.php/tckhdhdl/article/view/911 10.37569/DalatUniversity.11.4.911(2021) en Tạp chí Khoa học Đại học Đà Lạt, Tập 11, Số 4; tr. 45-54 application/pdf Trường Đại học Đà Lạt
institution Thư viện Trường Đại học Đà Lạt
collection Thư viện số
language English
description We synthesized 0-3 type (1-x)PbTiO3-xNiFe2O4 (x = 0.0-0.5) multiferroic composites with two independently crystallized parent phases by the sol-gel method. Structural, surface morphology, vibrational, optical, and magnetic characteristics were investigated by X-ray diffraction (XRD), SEM, Raman scattering, UV-vis absorption, and magnetization (M-H) measurements, respectively. The XRD result showed that the lattice parameter a of the PbTiO3 (PTO) phase decreased while lattice parameter c increased after compositing, leading to a decrease in the tetragonal ratio c/a. SEM images indicated that the NiFe2O4 (NFO) crystals that crystallized later are small and adhere to the surface of the large PTO particles. The strong cohesion between the two components was also revealed by the gradual shift of the Raman peaks to the lower wavelength and the reduction of the Raman intensity as the NFO content increased. The UV-vis absorption result showed the co-absorption spectra of the parent phases in the composites. Magnetization curves presented a sharp increase in saturation magnetization MS with NFO content from 0.014 emu/g for the PTO sample to 14.360 emu/g for the composite containing 50 mol% NFO. This study indicates an effective method in the search for multilayer composites.
format Article
author Pham, Do Chung
Le, Thi Mai Oanh
Nguyen, Van Minh
spellingShingle Pham, Do Chung
Le, Thi Mai Oanh
Nguyen, Van Minh
STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES
author_facet Pham, Do Chung
Le, Thi Mai Oanh
Nguyen, Van Minh
author_sort Pham, Do Chung
title STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES
title_short STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES
title_full STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES
title_fullStr STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES
title_full_unstemmed STRUCTURAL, VIBRATIONAL, OPTICAL, AND MAGNETIC PROPERTIES OF 0-3 TYPE PARTICULATE PbTiO3-NiFe2O4 COMPOSITES
title_sort structural, vibrational, optical, and magnetic properties of 0-3 type particulate pbtio3-nife2o4 composites
publisher Trường Đại học Đà Lạt
publishDate 2023
url https://scholar.dlu.edu.vn/thuvienso/handle/DLU123456789/114424
https://tckh.dlu.edu.vn/index.php/tckhdhdl/article/view/911
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